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Dispersion of Highly Filled Thermosets – Part Ten: Measuring Fineness of Grind Using a Hegman Gage

March 25, 2019 By Jeffrey Gotro 1 Comment

Previous nine posts covered many of the mechanical aspects of dispersing fillers into thermoset resins.  The final post in this series will cover measuring the mixing effectiveness using the fineness of grind or the Hegman gage.  The Hegman gage is commonly used as a quality control test at the end of a mixing process.  A small amount of material is required and can be obtained ... [Click to Continue...]

Dispersion of Highly Filled Thermosets – Part Nine: Efficacy of Sweeper Blades During Mixing

March 11, 2019 By Jeffrey Gotro 2 Comments

Previous posts have covered the various types of mixing geometries such as single, dual and triple shaft mixers and double planetary mixers.  The focus was on understanding the mixing physics.  There are several ways to improve the efficacy of the mixing process.  The last post covered the use of vacuum to accelerate degassing during the mixing process.  This post will discuss ... [Click to Continue...]

Dispersion of Highly Filled Thermosets – Part Eight: Vacuum Degassing

March 4, 2019 By Jeffrey Gotro Leave a Comment

The previous posts have focused on the mechanics of the mixing process and have briefly covered the use of vacuum during mixing.  This post will discuss vacuum degassing in detail. Many commercially important, highly-filled formulations require effective vacuum mixing to achieve the desired properties.  Many liquid or viscous thermoset resins need to be degassed prior to ... [Click to Continue...]

Dispersion of Highly Filled Thermosets – Part Seven: Dual Axis Centrifugal Laboratory Mixers

February 25, 2019 By Jeffrey Gotro 2 Comments

The first six posts in this series covered the various types of equipment used to disperse fillers into uncured thermoset resins.  The information was applicable to all sizes of mixing equipment.  This post will focus on laboratory size mixers for use during formulation development and testing.  In the formulation phase, multiple iterations are typically required to optimize ... [Click to Continue...]

To Mix or Mill: Thick Film Paste and Ink

February 18, 2019 By Jeffrey Gotro 1 Comment

Guest Post by Ken Kuang, Torrey Hills Technologies Introduction Thick Film Material is an ink paste produced through dispersing metal powders, glass powders, and inorganic oxides with organic solvent in a three-roll mill.  The thick film pastes are screen-printed on ceramic boards or green sheets as circuit patterns and then fired at high temperatures. The thick film ... [Click to Continue...]

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Polymer Innovation Blog

I’m Dr. Jeff Gotro and welcome to the Polymer Innovation Blog. Over the last 40 years I have been involved in polymer research, along with product and process development. I acquired invaluable experience working for IBM, AlliedSignal, Honeywell, Ablestik Labs (now Henkel) and in multiple consulting projects. In this blog, I (along with some guest contributors) will share our experiences, tips, and “tricks of the trade” to get more out of your innovation efforts and discuss new trends and technical advances in the polymer industry.
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Polymers in Electronic Packaging

polymers in electronic packaging Are you confused about what is electronic packaging? Have you ever wondered what type of polymers and polymer-based composites are used in electronics? Learn More...

Practical Tips for Curing Thermosets

practical tips for curing thermosets Have you ever had a question about the degree of cure or is your part fully cured after processing? Confused about what is gelation or how does vitrification impact thermoset curing? Learn More...

Rheology of Thermosets

rheology of thermosets Have you ever had a question about measuring the rheological properties of thermosets Didn’t know what is the right experimental approach to get the right rheological information? Learn More...

Dielectric Cure Monitoring of Thermosets

Dielectric Cure Monitoring of Thermosets Do you have a need for an in-situ cure monitor for a thermoset process but don’t know where to start? Are you confused about the terminology used in dielectric spectroscopy? Learn More...

Introduction to Biopolymers and Bioplastics

Introduction to Biopolymers and Bioplastics Would you like to know how sustainable are bio-based polymers? Or what is the market size and growth rate for bioplastics? Or have questions about the biomass supply chain? Learn More...

Thermoset Characterization

Thermoset Characterization Have you ever had a question about how to measure a physical property of a thermoset? Confused about what is gelation or how does vitrification impact thermoset curing profiles? Or wondered how to measure the glass transition temperature of an epoxy or polyester composite? Learn More...

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